Distillation and separation modules

Functional process modules for heating, evaporation, separation, cooling, condensation and preparation of liquid, vapor and gas–liquid streams

Industrial distillation and separation modules

Modular construction of process lines

Distillation and separation processes can be formed from separate functional modules, each of which performs a specific process step: feed preparation, heating, evaporation, phase separation, cooling, condensation or collection of the output streams.

The modular approach can provide a new plant, extend an existing process line or replace individual equipment sections. The composition, sequence and design of the modules are determined by feed stream properties and the required output specifications.

Applications

Processing of petroleum products
Regeneration of used oils
Removing water and solvents
Stabilization of liquid hydrocarbon streams
Oil preparation
Preparation of gas-liquid streams
Condensate collection and separation
Drying solid and pasty residues
Laboratory and pilot studies
Modernization of existing installations

Main tasks of modules

Feed preparation

Feed receipt, storage, filtration, mixing and transfer to downstream stages

Controlled heating

Controlled heat input to a liquid or solid feed under the selected operating conditions

Evaporation of volatile components

Transfer of water, solvents or light fractions into the vapor phase

Phase separation

Separation of liquid, gas and solid phases in the sequence provided by the process flowsheet

Vapor cooling

Reducing the temperature of a vapor or vapor–gas stream before condensation

Condensation

Condensation of the target vapor components

Collection of output streams

Separate accumulation of the main product, water, organic condensate and solid impurities

Automated control

Monitoring process parameters, equipment status and safety interlocks

Advantages of modular design

Configured for the application

The equipment package is selected for feedstock properties and the required separation

Phased system development

Individual modules can be commissioned sequentially

Modernization of existing equipment

New functional modules can be integrated into an existing process line

Scalability

Capacity can be increased by selecting larger equipment or installing modules in parallel

Factory-built modules

Individual units can be supplied with piping, instrumentation and control system

Reduced on-site work

Pre-assembly of equipment reduces the amount of installation work on site

Ease of maintenance

Dividing the installation into functional sections simplifies access to individual components

Integrated automation

Control of individual modules can be combined into a common system

Process module options

The equipment package is selected taking into account the physical state of the product, temperature, pressure, water content, volatile components, mechanical impurities and requirements for the resulting process streams.

Feed receipt and preparation module
Pre-filtration module
Product heating module
Evaporation module
Distillation module
Working gas circulation module
Vapor–gas stream cooling module
Condensing module
Gas-liquid separation module
Liquid phase separation module
Condensate collection module
Final filtration module
Laboratory-scale process module
Pilot process plant
Industrial modular plant
Automated control module

Main stages of the process flowsheet

  1. Reception of the feedstock
  2. Sampling and characterization
  3. Pre-filtration if necessary
  4. Storage and equalization
  5. Feeding the product into the process unit
  6. Controlled heating
  7. Evaporation of target components
  8. Removal of vapor or vapor–gas stream
  9. Gas-liquid separation if necessary
  10. Flow cooling
  11. Vapor condensation
  12. Separation of liquid phases if necessary
  13. Collection of main product and condensate
  14. Return of working gas where a recirculation loop is included
  15. Testing the output streams

Not all of the steps listed apply simultaneously. The composition and sequence of modules are determined by a specific process requirement.

Feed preparation module

Before entering the main process units, the feed may need storage, equalization, removal of coarse solids and pre-filtration. The pretreatment section depends on the feed's physical properties and contamination level.

Receiving tank
Product accumulation
Feed equalization
Pre-settling
Mechanical filtration
Metered feed
Stirring as necessary
Preheating

Heating and evaporation module

The module provides a controlled supply of heat to the product and creates conditions for the evaporation of water, solvents or other volatile components. The operating mode is determined by the composition of the feed stream and the permissible processing temperature.

The design of the heating section and the method of heat transfer are selected individually. The equipment type is selected once the process flowsheet has been confirmed.

Controlled product heating
Maintaining the specified operating conditions
Water evaporation
Evaporation of solvents
Evaporation of light components
Temperature control
Overheat protection
Vapor outlet

Distillation module

The distillation module separates components by volatility. Lighter components vaporize and flow to the cooling and condensation section.

Feedstock testing determines the number of stages, operating temperatures and process arrangement. The module is configured for the application.

Feed supply
Controlled evaporation
Removal of light components
Collection of the main liquid fraction
Monitoring operating parameters
Connection to the condensation module

Separation modules

Separation modules are designed to separate gas, liquid and gas-liquid flows. The design and internal devices are selected taking into account the composition, flow rate, density and physical state of the separated phases.

Two-phase liquid-gas separation
Three-phase separation of oil, water and gas
Removal of entrained liquid droplets from a gas stream
Separation of mechanical impurities
Separation of aqueous and hydrocarbon phases
Condensate collection
Monitoring the level of liquid phases
Protective shutdowns where required

Cooling and condensation

The vapor or vapor–gas stream leaving the process unit enters the cooling system. Target components condense and are collected in receiving vessels.

The condensation module can work in conjunction with a gas-liquid separator and a liquid phase separation system. The equipment package is determined by the properties of the vapors and the requirements for the condensate.

Vapor stream cooling
Vapor–gas stream cooling
Water condensation
Condensation of organic components
Gas-liquid separation
Condensate collection
Liquid phase separation
Temperature and level control

Working gas circulation

In certain process flows, a working or inert gas may be used to transfer water vapor, solvents and other volatile components from the heated product to the cooling and condensation system.

Once the condensable components have been separated, the gas can be returned to the process. The type of gas, flow rate, pressure and circulation mode are determined by the project.

Working gas supply
Contact with the product
Vapor transfer
Gas flow cooling
Condensate separation
Return of gas to the process
Pressure control
Safety interlocks

Modular line equipment

Receiving and storage tanks
Pumping equipment
Pre-filters
Process equipment
Heating equipment
Heat exchangers
Coolers
Condensers
Gas-liquid separators
Liquid separation tanks
Condensate collectors
Working gas circulation system if necessary
Piping
Shut-off and control valves
Instrumentation and safety interlocks
Process control system

The final equipment package follows the approved process flow diagram. Individual items are used only when necessary.

Equipment configurations

Functional modules may be supplied as individual units, frame-mounted assemblies or parts of a complete plant. Their design depends on required throughput, site conditions and transport and installation constraints.

Lower-throughput laboratory and pilot units can be used to establish operating conditions and verify the process flowsheet.

Separate process unit
Frame-mounted module
Block-modular design
Containerized configuration where feasible
Laboratory-scale unit
Pilot-scale unit
Industrial plant
Integration into an existing process line
Phased expansion
Automated control

Resulting process streams

Primary liquid product

Liquid fraction after the processing provided by the process flowsheet and removal of some volatile components

Water condensate

Water separated from the feedstock and collected after cooling the vapor stream

Organic condensate

Solvents or light hydrocarbon components that become liquid after cooling

Gas stream

Gas after removal of entrained liquid droplets and condensable components

Solid impurities

Mechanical impurities and sediments separated at the preparatory or separation stages

Options and configurations

1

Feed preparation module

Reception, accumulation, filtration, mixing and supply of the feedstock

2

Heating and evaporation module

Equipment for controlled heat input and devolatilization

3

Distillation module

Process equipment and auxiliary equipment for separating components by volatility

4

Separation module

Equipment for separation of gas, liquid and solid phases

5

Condensing module

Coolers, condensers, separators and liquid collection tanks

6

Complete modular installation

Sequential integration of preparation, heating, separation, cooling, condensation and automated control

How modules are selected

  1. Review of project data
  2. Determination of the composition and physical state of the product
  3. Determination of water and volatile components
  4. Determination of mechanical impurities
  5. Temperature evaluation
  6. Determining the required separation
  7. Clarification of requirements for output streams
  8. Laboratory tests
  9. Pilot tests if necessary
  10. Selection of process stages
  11. Selection of individual modules
  12. Development of equipment connection diagram
  13. Control system selection
  14. Preparation of technical proposal

The final equipment package is selected after feedstock analysis. No single module is suitable for every process application.

Delivery and implementation

Review of project requirements
Study of product samples
Laboratory tests
Pilot tests if necessary
Development of a process flowsheet
Selecting the module package
Preparation of design input data
Design
Selection and configuration of equipment
Manufacturing of process modules
Factory assembly
Factory testing
Delivery
Installation or installation supervision
Commissioning
Optimization of operating conditions
Automation and safety system setup
Operator training
Acceptance tests
After-sales support

Available equipment configurations

Laboratory process units
Pilot distillation modules
Industrial evaporation modules
Gas-liquid separation modules
Liquid phase separation modules
Condensing modules
Condensate collection systems
Integrated modular plants

We will configure the process modules for your application

To prepare a technical solution, information is required on the feed composition and flow rate, physical state, water and volatile-component content, operating parameters, existing equipment and requirements for the output streams.