Distillation, regeneration and clarification of petroleum products

Modular installations for separation, dehydration, solvent regeneration and production of target fractions from heavy petroleum products

Industrial distillation and regeneration equipment

Separation and recovery of petroleum products

Process solutions are designed for the separation of complex liquid and paste-like petroleum products, removal of water and solvents, oil regeneration and the production of individual distillate fractions. In this process, circulating inert gas contacts the heated product and carries volatile vapors to the cooling and condensation stages.

Equipment and operating conditions are selected for the feedstock properties and target product specifications. The scope may include laboratory, pilot or industrial units, engineering documentation, equipment supply, integration into an existing plant and operational support.

Processed feedstock

Fuel oil and heavy oil products
Tar and residual petroleum products
Used motor and industrial oils
Extraction oils and residual extracts
Pyrolysis resins
Petroleum products with high water content
Petroleum products and post-extraction products containing solvents
Very high-viscosity and thermally unstable hydrocarbon mixtures

Benefits of technology

Closed inert gas circuit

Inert gas circulates inside the installation, transfers vapors of volatile components to the cooling and condensation unit, and then returns to the process

Operation without high vacuum

Operation without high vacuum may be feasible for selected feedstocks and target fractions, subject to process testing and engineering assessment

Controlled temperature

Heating evaporates and separates components without burning the feedstock. Operating conditions are selected to avoid thermal degradation of the feed components

Processing complex feedstocks

The process can be assessed for viscous and thermally unstable petroleum and petrochemical mixtures

Solvent recovery

The recovered solvent is condensed and can be returned to the process cycle

Product recovery

The process can recover distillate fractions, dehydrated petroleum products and a heavy residue whose properties depend on the feedstock and operating conditions

Modularity and scalability

The process solution can be tested in a laboratory and pilot plant and scaled to industrial implementation

Integration and automation

The equipment can be integrated into existing plants and fitted with process monitoring and control systems

Process configurations

The process flowsheet is tailored to feedstock properties and target specifications for the distillate fractions and heavy residue.

Obtaining distillates from fuel oil and tar
Regeneration of used motor and industrial oils
Dehydration of petroleum products and oil-containing waste
Removal and recovery of solvent residues
Clarification and improvement of the quality of dark petroleum products
Increase in flash point of heavy petroleum products
Increasing the viscosity of heavy residue and obtaining non-oxidized bitumen
Separation of extraction oils and residual extracts
Distillation and rectification modules

Main process stages

  1. Feed intake and pretreatment
  2. Controlled heating of the material being separated
  3. Product contact with circulating inert gas
  4. Evaporation of water, solvents and volatile components into the vapor–gas stream
  5. Cooling and condensation of extracted components
  6. Separation and collection of resulting liquid products
  7. Returning inert gas to the process loop
  8. Discharge of the treated product or heavy residue

The process sequence, operating temperatures and equipment package depend on feedstock properties and target product specifications.

Modular and scalable design

The process train combines feed and heating units, inert-gas contact, cooling, condensation, separation, gas recirculation and product collection. The equipment package is specified after feedstock testing and process calculations.

Plants can be configured for laboratory, pilot, demonstration-scale or industrial use. They can operate as stand-alone systems or be integrated into or used to upgrade an existing line.

Laboratory-scale unitPilot-scale unitDemonstration plantIndustrial modular plantIntegration into an existing plantModernization of existing equipment

Recovered products

Distillate fractions

Light and medium fractions recovered from the heavy feedstock and sent for further use or additional processing

Recovered solvent

Solvent separated from a product by evaporation and condensation and returned to the process cycle when it meets the required characteristics

Dehydrated petroleum product

Petroleum product with reduced content of water, solvent and light components, prepared for further use or processing

Heavy residue to specification

Stabilized heavy product with specified viscosity and flash point, including the possibility of obtaining non-oxidized bitumen

Options and configurations

1

Laboratory-scale unit

Testing feedstock separation and determining operating temperatures, inert-gas flow rate and distillate composition

2

Pilot-scale unit

Testing the process flowsheet with a larger feedstock volume and collecting scale-up data

3

Industrial modular plant

A set of equipment for continuous or batch processing of a product with the required throughput

4

Integration into an existing plant

Separate process modules for modernization of existing plants and oil refineries

How a process flowsheet is selected

  1. Review of project data
  2. Collecting and analyzing a feedstock sample
  3. Determination of the composition and basic properties of the product
  4. Laboratory separation and analysis of the resulting fractions
  5. Pilot tests if necessary
  6. Selection of operating temperature, inert-gas flow rate and condensation conditions
  7. Scale-up assessment and equipment package selection
  8. Preparation of technical proposal and design input data

The final process flowsheet is based on feedstock analysis. Laboratory and pilot testing may be required for complex, viscous and unstable mixtures.

Engineering and plant upgrades

The technology can be used both as part of a stand-alone installation and in the modernization of existing oil refining and petrochemical plants.

Increased yield of light petroleum products

Recovery of additional distillate fractions from heavy streams and residues

Improving the quality of heavy products

Removal of water and excess light hydrocarbons, raising flash point and stabilizing product

Obtaining a heavy residue with specified properties

Increasing the viscosity of the residual product and the possibility of obtaining non-oxidized bitumen

Modernization of existing equipment

Development of initial data, design and engineering documentation for new process units and modernization of existing installations

Actual performance depends on feedstock properties, the existing process and the results of engineering calculations and tests.

Delivery and implementation

Applied research
Laboratory research
Pilot testing
Development of a process solution
Development of design input data
Development of project documentation
Development of design documentation
Manufacturing and supply of equipment
Installation and commissioning
Optimization of operating conditions
Operator training
Operational support

Available equipment configurations

Laboratory and pilot plants
Industrial distillation equipment
Equipment for producing distillates from fuel oil and tar
Equipment for dehydration and solvent recovery
Modernization of oil refineries
Research and scale-up

We will develop a process flowsheet for your feedstock and target products

To develop a technical proposal, we need the feedstock composition, required throughput, details of existing equipment and target properties of the distillate fractions.